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. Author manuscript; available in PMC: 2016 Mar 3.
Published in final edited form as: Carbohydr Res. 2016 Jan 5;422:5–12. doi: 10.1016/j.carres.2015.12.009

Table 1.

13C NMR chemical shifts (δ) of compounds 10, 16 and 19

Residue Carbon 10 16 19
→4,5)-α-Kdop
1 176.05 175.94 176.05b
2 101.35 101.35 101.34
3 35.24 35.21 35.19
4 72.12 72.04a 72.04c
5 74.47 73.94 73.78
6 73.22 73.11 73.10
7 69.26 69.35 69.29
8 63.98 64.00 64.08
α-Kdop-(2→4)-
1 176.05 176.03 175.92b
2 102.87 102.82 102.84
3 35.42 35.48 35.50
4 66.67 66.73 66.75
5 67.68 67.66 67.67
6 72.50 72.55 72.55d
7 71.52 71.50 71.52
8 63.58 63.82 63.63
α-Glcp-(1→5)-
1 100.31 99.72 99.61
2 72.88 72.60 72.45
3 73.29 71.90a 72.03c
4 69.76 79.07 79.98
5 72.64 71.25 71.06
6 60.69 60.29 60.30
β-Glcp-(1→4)-
1 103.36 103.69
2 73.94 73.81
3 76.33 76.40
4 70.33 70.49
5 76.78 74.97
6 61.46 66.74
α-Glcp-(1→6)-
1 98.79
2 72.32
3 73.62
4 70.49
5 72.71d
6 61.39
OCH3 51.37 51.38 51.37
a-d

Assigments within a column may be reversed