O3—C2 | 1.344 (3) | C3—C4 | 1.472 (3) |
O3—H1O3 | 0.97 (4) | C6—C7 | 1.387 (3) |
O1—C1 | 1.230 (2) | C6—H6 | 0.93 |
O2—C4 | 1.228 (2) | C8—C7 | 1.387 (3) |
C10—C9 | 1.333 (3) | C8—H8 | 0.93 |
C10—C22 | 1.496 (3) | C7—H7 | 0.93 |
C10—C12 | 1.501 (3) | C12—H12A | 0.96 |
C9—C3 | 1.472 (3) | C12—H12B | 0.96 |
C9—H9 | 0.93 | C12—H12C | 0.96 |
C4A—C5 | 1.389 (3) | C12—H12D | 0.96 |
C4A—C8A | 1.398 (3) | C12—H12E | 0.96 |
C4A—C4 | 1.498 (3) | C12—H12F | 0.96 |
C8A—C8 | 1.398 (3) | C22—H22A | 0.96 |
C8A—C1 | 1.469 (3) | C22—H22B | 0.96 |
C2—C3 | 1.361 (3) | C22—H22C | 0.96 |
C2—C1 | 1.485 (3) | C22—H22D | 0.96 |
C5—C6 | 1.390 (3) | C22—H22E | 0.96 |
C5—H5 | 0.93 | C22—H22F | 0.96 |
C2—O3—H1O3 | 108.3 (18) | C10—C12—H12C | 109.5 |
C9—C10—C22 | 124.9 (2) | H12A—C12—H12C | 109.5 |
C9—C10—C12 | 120.2 (2) | H12B—C12—H12C | 109.5 |
C22—C10—C12 | 114.91 (19) | C10—C12—H12D | 109.5 |
C10—C9—C3 | 127.1 (2) | H12A—C12—H12D | 141.1 |
C10—C9—H9 | 116.5 | H12B—C12—H12D | 56.3 |
C3—C9—H9 | 116.5 | H12C—C12—H12D | 56.3 |
C5—C4A—C8A | 119.67 (19) | C10—C12—H12E | 109.5 |
C5—C4A—C4 | 120.09 (19) | H12A—C12—H12E | 56.3 |
C8A—C4A—C4 | 120.23 (18) | H12B—C12—H12E | 141.1 |
C4A—C8A—C8 | 120.21 (19) | H12C—C12—H12E | 56.3 |
C4A—C8A—C1 | 119.46 (19) | H12D—C12—H12E | 109.5 |
C8—C8A—C1 | 120.32 (19) | C10—C12—H12F | 109.5 |
O3—C2—C3 | 121.45 (19) | H12A—C12—H12F | 56.3 |
O3—C2—C1 | 115.56 (18) | H12B—C12—H12F | 56.3 |
C3—C2—C1 | 122.95 (19) | H12C—C12—H12F | 141.1 |
O1—C1—C8A | 122.31 (19) | H12D—C12—H12F | 109.5 |
O1—C1—C2 | 119.00 (18) | H12E—C12—H12F | 109.5 |
C8A—C1—C2 | 118.68 (18) | C10—C22—H22A | 109.5 |
C4A—C5—C6 | 119.8 (2) | C10—C22—H22B | 109.5 |
C4A—C5—H5 | 120.1 | H22A—C22—H22B | 109.5 |
C6—C5—H5 | 120.1 | C10—C22—H22C | 109.5 |
C2—C3—C4 | 118.61 (19) | H22A—C22—H22C | 109.5 |
C2—C3—C9 | 123.83 (19) | H22B—C22—H22C | 109.5 |
C4—C3—C9 | 117.35 (18) | C10—C22—H22D | 109.5 |
O2—C4—C3 | 120.66 (19) | H22A—C22—H22D | 141.1 |
O2—C4—C4A | 119.58 (18) | H22B—C22—H22D | 56.3 |
C3—C4—C4A | 119.76 (18) | H22C—C22—H22D | 56.3 |
C7—C6—C5 | 120.7 (2) | C10—C22—H22E | 109.5 |
C7—C6—H6 | 119.6 | H22A—C22—H22E | 56.3 |
C5—C6—H6 | 119.6 | H22B—C22—H22E | 141.1 |
C7—C8—C8A | 119.7 (2) | H22C—C22—H22E | 56.3 |
C7—C8—H8 | 120.2 | H22D—C22—H22E | 109.5 |
C8A—C8—H8 | 120.2 | C10—C22—H22F | 109.5 |
C6—C7—C8 | 119.9 (2) | H22A—C22—H22F | 56.3 |
C6—C7—H7 | 120 | H22B—C22—H22F | 56.3 |
C8—C7—H7 | 120 | H22C—C22—H22F | 141.1 |
C10—C12—H12A | 109.5 | H22D—C22—H22F | 109.5 |
C10—C12—H12B | 109.5 | H22E—C22—H22F | 109.5 |
H12A—C12—H12B | 109.5 | ||
O1—C1—C2—O3 | 0.2 (3) | O2—C4—C4A—C5 | 2.6 (3) |
O1—C1—C2—C3 | −177.5 (2) | O2—C4—C4A—C8A | −176.8 (2) |
C8A—C1—C2—O3 | 179.69 (19) | C3—C4—C4A—C5 | −177.0 (2) |
C8A—C1—C2—C3 | 2.0 (3) | C3—C4—C4A—C8A | 3.5 (3) |
O1—C1—C8A—C4A | 175.2 (2) | C4—C4A—C5—C6 | 179.6 (2) |
O1—C1—C8A—C8 | −3.9 (3) | C8A—C4A—C5—C6 | −1.0 (3) |
C2—C1—C8A—C4A | −4.3 (3) | C4—C4A—C8A—C1 | 1.6 (3) |
C2—C1—C8A—C8 | 176.6 (2) | C4—C4A—C8A—C8 | −179.4 (2) |
O3—C2—C3—C4 | −174.50 (19) | C5—C4A—C8A—C1 | −177.9 (2) |
O3—C2—C3—C9 | 0.2 (3) | C5—C4A—C8A—C8 | 1.2 (3) |
C1—C2—C3—C4 | 3.1 (3) | C4A—C5—C6—C7 | −0.4 (3) |
C1—C2—C3—C9 | 177.8 (2) | C5—C6—C7—C8 | 1.5 (3) |
C2—C3—C4—O2 | 174.5 (2) | C6—C7—C8—C8A | −1.3 (3) |
C2—C3—C4—C4A | −5.9 (3) | C7—C8—C8A—C1 | 179.0 (2) |
C9—C3—C4—O2 | −0.5 (3) | C7—C8—C8A—C4A | −0.1 (3) |
C9—C3—C4—C4A | 179.15 (19) | C3—C9—C10—C12 | −176.6 (2) |
C2—C3—C9—C10 | 50.7 (3) | C3—C9—C10—C22 | 4.9 (4) |
C4—C3—C9—C10 | −134.6 (2) |