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. 2016 Jan 16;72(Pt 2):188–190. doi: 10.1107/S2056989015024755
O3—C2 1.344 (3) C3—C4 1.472 (3)
O3—H1O3 0.97 (4) C6—C7 1.387 (3)
O1—C1 1.230 (2) C6—H6 0.93
O2—C4 1.228 (2) C8—C7 1.387 (3)
C10—C9 1.333 (3) C8—H8 0.93
C10—C22 1.496 (3) C7—H7 0.93
C10—C12 1.501 (3) C12—H12A 0.96
C9—C3 1.472 (3) C12—H12B 0.96
C9—H9 0.93 C12—H12C 0.96
C4A—C5 1.389 (3) C12—H12D 0.96
C4A—C8A 1.398 (3) C12—H12E 0.96
C4A—C4 1.498 (3) C12—H12F 0.96
C8A—C8 1.398 (3) C22—H22A 0.96
C8A—C1 1.469 (3) C22—H22B 0.96
C2—C3 1.361 (3) C22—H22C 0.96
C2—C1 1.485 (3) C22—H22D 0.96
C5—C6 1.390 (3) C22—H22E 0.96
C5—H5 0.93 C22—H22F 0.96
C2—O3—H1O3 108.3 (18) C10—C12—H12C 109.5
C9—C10—C22 124.9 (2) H12A—C12—H12C 109.5
C9—C10—C12 120.2 (2) H12B—C12—H12C 109.5
C22—C10—C12 114.91 (19) C10—C12—H12D 109.5
C10—C9—C3 127.1 (2) H12A—C12—H12D 141.1
C10—C9—H9 116.5 H12B—C12—H12D 56.3
C3—C9—H9 116.5 H12C—C12—H12D 56.3
C5—C4A—C8A 119.67 (19) C10—C12—H12E 109.5
C5—C4A—C4 120.09 (19) H12A—C12—H12E 56.3
C8A—C4A—C4 120.23 (18) H12B—C12—H12E 141.1
C4A—C8A—C8 120.21 (19) H12C—C12—H12E 56.3
C4A—C8A—C1 119.46 (19) H12D—C12—H12E 109.5
C8—C8A—C1 120.32 (19) C10—C12—H12F 109.5
O3—C2—C3 121.45 (19) H12A—C12—H12F 56.3
O3—C2—C1 115.56 (18) H12B—C12—H12F 56.3
C3—C2—C1 122.95 (19) H12C—C12—H12F 141.1
O1—C1—C8A 122.31 (19) H12D—C12—H12F 109.5
O1—C1—C2 119.00 (18) H12E—C12—H12F 109.5
C8A—C1—C2 118.68 (18) C10—C22—H22A 109.5
C4A—C5—C6 119.8 (2) C10—C22—H22B 109.5
C4A—C5—H5 120.1 H22A—C22—H22B 109.5
C6—C5—H5 120.1 C10—C22—H22C 109.5
C2—C3—C4 118.61 (19) H22A—C22—H22C 109.5
C2—C3—C9 123.83 (19) H22B—C22—H22C 109.5
C4—C3—C9 117.35 (18) C10—C22—H22D 109.5
O2—C4—C3 120.66 (19) H22A—C22—H22D 141.1
O2—C4—C4A 119.58 (18) H22B—C22—H22D 56.3
C3—C4—C4A 119.76 (18) H22C—C22—H22D 56.3
C7—C6—C5 120.7 (2) C10—C22—H22E 109.5
C7—C6—H6 119.6 H22A—C22—H22E 56.3
C5—C6—H6 119.6 H22B—C22—H22E 141.1
C7—C8—C8A 119.7 (2) H22C—C22—H22E 56.3
C7—C8—H8 120.2 H22D—C22—H22E 109.5
C8A—C8—H8 120.2 C10—C22—H22F 109.5
C6—C7—C8 119.9 (2) H22A—C22—H22F 56.3
C6—C7—H7 120 H22B—C22—H22F 56.3
C8—C7—H7 120 H22C—C22—H22F 141.1
C10—C12—H12A 109.5 H22D—C22—H22F 109.5
C10—C12—H12B 109.5 H22E—C22—H22F 109.5
H12A—C12—H12B 109.5
O1—C1—C2—O3 0.2 (3) O2—C4—C4A—C5 2.6 (3)
O1—C1—C2—C3 −177.5 (2) O2—C4—C4A—C8A −176.8 (2)
C8A—C1—C2—O3 179.69 (19) C3—C4—C4A—C5 −177.0 (2)
C8A—C1—C2—C3 2.0 (3) C3—C4—C4A—C8A 3.5 (3)
O1—C1—C8A—C4A 175.2 (2) C4—C4A—C5—C6 179.6 (2)
O1—C1—C8A—C8 −3.9 (3) C8A—C4A—C5—C6 −1.0 (3)
C2—C1—C8A—C4A −4.3 (3) C4—C4A—C8A—C1 1.6 (3)
C2—C1—C8A—C8 176.6 (2) C4—C4A—C8A—C8 −179.4 (2)
O3—C2—C3—C4 −174.50 (19) C5—C4A—C8A—C1 −177.9 (2)
O3—C2—C3—C9 0.2 (3) C5—C4A—C8A—C8 1.2 (3)
C1—C2—C3—C4 3.1 (3) C4A—C5—C6—C7 −0.4 (3)
C1—C2—C3—C9 177.8 (2) C5—C6—C7—C8 1.5 (3)
C2—C3—C4—O2 174.5 (2) C6—C7—C8—C8A −1.3 (3)
C2—C3—C4—C4A −5.9 (3) C7—C8—C8A—C1 179.0 (2)
C9—C3—C4—O2 −0.5 (3) C7—C8—C8A—C4A −0.1 (3)
C9—C3—C4—C4A 179.15 (19) C3—C9—C10—C12 −176.6 (2)
C2—C3—C9—C10 50.7 (3) C3—C9—C10—C22 4.9 (4)
C4—C3—C9—C10 −134.6 (2)