| Nonius KappaCCD diffractometer | 1802 reflections with I > 2σ(I) |
| Radiation source: Enraf-Nonius FR590 | Rint = 0.041 |
| Graphite monochromator | θmax = 27.5°, θmin = 2.6° |
| Detector resolution: 9 pixels mm-1 | h = −5→5 |
| CCD rotation images, thick slices scans | k = −19→21 |
| 4661 measured reflections | l = −20→20 |
| 2585 independent reflections |
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