| Refinement on F2 | 138 restraints |
| Least-squares matrix: full | Hydrogen site location: inferred from neighbouring sites |
| R[F2 > 2σ(F2)] = 0.054 | H-atom parameters constrained |
| wR(F2) = 0.155 | w = 1/[σ2(Fo2) + (0.0732P)2 + 3.5911P] where P = (Fo2 + 2Fc2)/3 |
| S = 1.02 | (Δ/σ)max = 0.001 |
| 15805 reflections | Δρmax = 1.17 e Å−3 |
| 965 parameters | Δρmin = −0.86 e Å−3 |