| Crystal data |
| Chemical formula |
[Zn(C72H44N4O8)(C6H4N2)]·C6H4N2
|
|
M
r
|
1366.70 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
11.8587 (3), 16.1619 (5), 19.2167 (5) |
| α, β, γ (°) |
68.207 (3), 81.077 (2), 86.866 (2) |
|
V (Å3) |
3378.43 (18) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.43 |
| Crystal size (mm) |
0.38 × 0.13 × 0.07 |
| |
| Data collection |
| Diffractometer |
Agilent Xcalibur, Eos, Gemini ultra |
| Absorption correction |
Multi-scan (CrysAlis PRO; Agilent, 2014 ▸) |
|
T
min, T
max
|
0.830, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
37755, 15805, 11876 |
|
R
int
|
0.029 |
| (sin θ/λ)max (Å−1) |
0.693 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.054, 0.155, 1.02 |
| No. of reflections |
15805 |
| No. of parameters |
965 |
| No. of restraints |
138 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
1.17, −0.86 |
