Table 1. Data collection and processing.
Values in parentheses are for the outer shell.
| HMP-1N–HMP-236–79 | HMP-1M | |
|---|---|---|
| Wavelength (Å) | 1.0332 | 0.97934 |
| Detector | Pilatus 6M | ADSC Q270 |
| Crystal-to-detector distance (mm) | 300 | 300 |
| Total rotation range (°) | 100 | 140 |
| Space group | P3121 | P212121 |
| a, b, c (Å) | 57.1, 57.1, 155.4 | 72.8, 81.5, 151.4 |
| α, β, γ (°) | 90, 90, 120 | 90, 90, 90 |
| Resolution range (Å) | 40–1.6 (1.67–1.60) | 40–2.4 (2.49–2.40) |
| No. of unique reflections | 39608 (3775) | 35766 (3683) |
| Completeness (%) | 99.7 (99.0) | 99.4 (98.9) |
| Multiplicity | 5.3 (5.0) | 3.9 (3.8) |
| Solvent content (%) | 40 | 54 |
| 〈I/σ(I)〉 | 24.3 (3.7) | 13.4 (5.3) |
| R merge † | 0.027 (0.36) | 0.085 (0.26) |
| CC1/2 ‡ | 0.999 (0.886) | 0.997 (0.911) |
| Overall B factor from Wilson plot (Å2) | 29.4 | 26.8 |
†
R
merge = 
, where I
i(hkl) is the ith measurement of reflection hkl and 〈I(hkl)〉 is the weighted mean of all measurements of I(hkl).
‡
CC1/2 is the Pearson correlation coefficient between random half data sets (Diederichs & Karplus, 2013 ▸).