Table 2. Experimental details.
| Crystal data | |
| Chemical formula | [Re(C10H6NO2)(C7H11N)(CO)3] |
| M r | 551.55 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 170 |
| a, b, c (Å) | 7.1529 (1), 29.5703 (5), 9.6309 (2) |
| β (°) | 105.572 (1) |
| V (Å3) | 1962.29 (6) |
| Z | 4 |
| Radiation type | Cu Kα |
| μ (mm−1) | 12.41 |
| Crystal size (mm) | 0.49 × 0.12 × 0.04 |
| Data collection | |
| Diffractometer | Rigaku R-AXIS SPIDER IPDS |
| Absorption correction | Multi-scan (CrystalClear; Rigaku 2005 ▸) |
| T min, T max | 0.374, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 21436, 3283, 2723 |
| R int | 0.069 |
| (sin θ/λ)max (Å−1) | 0.588 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.038, 0.102, 1.17 |
| No. of reflections | 3283 |
| No. of parameters | 253 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 1.30, −1.43 |