| Crystal data |
| Chemical formula |
C28H23FN4O·C2H6O |
|
M
r
|
496.57 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
297 |
|
a, b, c (Å) |
9.9754 (8), 10.2139 (8), 14.0294 (11) |
| α, β, γ (°) |
75.7386 (15), 71.0062 (14), 83.1264 (14) |
|
V (Å3) |
1308.73 (18) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.09 |
| Crystal size (mm) |
0.42 × 0.22 × 0.22 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII DUO CCD area detector |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2009 ▸) |
|
T
min, T
max
|
0.884, 0.955 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
32072, 5778, 3733 |
|
R
int
|
0.032 |
| (sin θ/λ)max (Å−1) |
0.650 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.057, 0.130, 1.21 |
| No. of reflections |
5778 |
| No. of parameters |
375 |
| No. of restraints |
3 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.15, −0.19 |
