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. 2016 Feb 20;72(Pt 3):382–386. doi: 10.1107/S205698901600267X
O11B—C11B 1.272 (2) C4A—H41A 0.9900
O12B—C11B 1.245 (2) C5A—H52A 0.9900
N1A—C11A 1.471 (2) C5A—H51A 0.9900
N1A—C7A 1.319 (2) C6A—H61A 0.9900
N1A—C2A 1.472 (2) C6A—H62A 0.9900
N8A—C7A 1.317 (2) C9A—H91A 0.9900
N8A—C9A 1.459 (2) C9A—H92A 0.9900
N8A—H8A 0.892 (18) C10A—H10A 0.9900
N4B—C4B 1.363 (2) C10A—H13A 0.9900
N4B—H41B 0.892 (18) C11A—H12A 0.9900
N4B—H42B 0.916 (17) C11A—H11A 0.9900
C2A—C3A 1.513 (3) C1B—C11B 1.499 (2)
C3A—C4A 1.526 (3) C1B—C2B 1.397 (2)
C4A—C5A 1.520 (3) C1B—C6B 1.394 (2)
C5A—C6A 1.533 (2) C2B—C3B 1.379 (2)
C6A—C7A 1.499 (2) C3B—C4B 1.402 (2)
C9A—C10A 1.509 (2) C4B—C5B 1.404 (2)
C10A—C11A 1.513 (2) C5B—C6B 1.380 (2)
C2A—H21A 0.9900 C2B—H2B 0.9500
C2A—H22A 0.9900 C3B—H3B 0.9500
C3A—H31A 0.9900 C5B—H5B 0.9500
C3A—H32A 0.9900 C6B—H6B 0.9500
C4A—H42A 0.9900
C2A—N1A—C7A 121.49 (15) C5A—C6A—H62A 109.00
C2A—N1A—C11A 117.17 (14) H61A—C6A—H62A 108.00
C7A—N1A—C11A 121.26 (15) C7A—C6A—H62A 109.00
C7A—N8A—C9A 122.97 (15) C7A—C6A—H61A 109.00
C7A—N8A—H8A 119.3 (11) C10A—C9A—H91A 110.00
C9A—N8A—H8A 117.8 (12) N8A—C9A—H92A 110.00
C4B—N4B—H41B 120.9 (13) N8A—C9A—H91A 110.00
H41B—N4B—H42B 114.5 (17) C10A—C9A—H92A 110.00
C4B—N4B—H42B 121.5 (13) H91A—C9A—H92A 108.00
N1A—C2A—C3A 113.83 (14) C9A—C10A—H10A 110.00
C2A—C3A—C4A 114.02 (15) H10A—C10A—H13A 108.00
C3A—C4A—C5A 114.29 (15) C9A—C10A—H13A 110.00
C4A—C5A—C6A 114.26 (14) C11A—C10A—H10A 110.00
C5A—C6A—C7A 111.90 (14) C11A—C10A—H13A 110.00
N8A—C7A—C6A 117.38 (15) N1A—C11A—H11A 110.00
N1A—C7A—N8A 122.23 (16) N1A—C11A—H12A 110.00
N1A—C7A—C6A 120.28 (15) C10A—C11A—H11A 110.00
N8A—C9A—C10A 108.79 (14) H11A—C11A—H12A 108.00
C9A—C10A—C11A 109.93 (14) C10A—C11A—H12A 110.00
N1A—C11A—C10A 109.88 (14) C6B—C1B—C11B 120.58 (15)
C3A—C2A—H22A 109.00 C2B—C1B—C11B 122.25 (15)
H21A—C2A—H22A 108.00 C2B—C1B—C6B 117.12 (15)
N1A—C2A—H22A 109.00 C1B—C2B—C3B 121.59 (15)
C3A—C2A—H21A 109.00 C2B—C3B—C4B 121.17 (15)
N1A—C2A—H21A 109.00 N4B—C4B—C3B 121.61 (16)
C2A—C3A—H31A 109.00 N4B—C4B—C5B 121.03 (16)
C2A—C3A—H32A 109.00 C3B—C4B—C5B 117.36 (15)
H31A—C3A—H32A 108.00 C4B—C5B—C6B 120.75 (16)
C4A—C3A—H31A 109.00 C1B—C6B—C5B 122.00 (16)
C4A—C3A—H32A 109.00 O11B—C11B—O12B 123.50 (17)
C3A—C4A—H42A 109.00 O11B—C11B—C1B 116.76 (16)
H41A—C4A—H42A 108.00 O12B—C11B—C1B 119.74 (17)
C5A—C4A—H41A 109.00 C1B—C2B—H2B 119.00
C5A—C4A—H42A 109.00 C3B—C2B—H2B 119.00
C3A—C4A—H41A 109.00 C2B—C3B—H3B 119.00
C6A—C5A—H52A 109.00 C4B—C3B—H3B 119.00
H51A—C5A—H52A 108.00 C4B—C5B—H5B 120.00
C4A—C5A—H52A 109.00 C6B—C5B—H5B 120.00
C6A—C5A—H51A 109.00 C1B—C6B—H6B 119.00
C4A—C5A—H51A 109.00 C5B—C6B—H6B 119.00
C5A—C6A—H61A 109.00
C7A—N1A—C2A—C3A −74.8 (2) N8A—C9A—C10A—C11A 52.82 (18)
C11A—N1A—C2A—C3A 108.53 (17) C9A—C10A—C11A—N1A −52.69 (19)
C2A—N1A—C7A—N8A −173.67 (15) C6B—C1B—C2B—C3B 1.0 (2)
C2A—N1A—C7A—C6A 10.2 (2) C11B—C1B—C2B—C3B 178.48 (15)
C11A—N1A—C7A—N8A 2.9 (3) C2B—C1B—C6B—C5B 0.1 (2)
C11A—N1A—C7A—C6A −173.23 (15) C11B—C1B—C6B—C5B −177.44 (15)
C2A—N1A—C11A—C10A −157.91 (14) C2B—C1B—C11B—O11B 179.25 (15)
C7A—N1A—C11A—C10A 25.4 (2) C2B—C1B—C11B—O12B −1.6 (3)
C9A—N8A—C7A—N1A −2.2 (3) C6B—C1B—C11B—O11B −3.4 (2)
C9A—N8A—C7A—C6A 174.06 (15) C6B—C1B—C11B—O12B 175.83 (16)
C7A—N8A—C9A—C10A −26.7 (2) C1B—C2B—C3B—C4B −0.9 (2)
N1A—C2A—C3A—C4A 77.87 (18) C2B—C3B—C4B—N4B 178.92 (16)
C2A—C3A—C4A—C5A −56.71 (19) C2B—C3B—C4B—C5B −0.4 (2)
C3A—C4A—C5A—C6A 62.97 (19) N4B—C4B—C5B—C6B −177.86 (16)
C4A—C5A—C6A—C7A −83.76 (18) C3B—C4B—C5B—C6B 1.4 (2)
C5A—C6A—C7A—N1A 60.9 (2) C4B—C5B—C6B—C1B −1.3 (3)
C5A—C6A—C7A—N8A −115.39 (17)