Oxford Diffraction Gemini-S CCD-detector diffractometer | 3324 independent reflections |
Radiation source: Enhance (Mo) X-ray source | 2847 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.031 |
Detector resolution: 16.067 pixels mm-1 | θmax = 29.2°, θmin = 3.3° |
ω scans | h = −10→10 |
Absorption correction: multi-scan (CrysAlis PRO; Agilent, 2014) | k = −16→15 |
Tmin = 0.93, Tmax = 0.99 | l = −17→18 |
7372 measured reflections |