| Oxford Diffraction Gemini-S CCD-detector diffractometer | 3311 independent reflections |
| Radiation source: fine-focus sealed tube | 2561 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.024 |
| Detector resolution: 16.077 pixels mm-1 | θmax = 26.0°, θmin = 3.4° |
| ω scans | h = −7→7 |
| Absorption correction: multi-scan (CrysAlis PRO; Agilent, 2014) | k = −14→24 |
| Tmin = 0.90, Tmax = 0.99 | l = −9→17 |
| 7082 measured reflections |
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