Oxford Diffraction Gemini-S CCD-detector diffractometer | 3339 independent reflections |
Radiation source: Enhance (Mo) X-ray source | 2347 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.034 |
Detector resolution: 16.077 pixels mm-1 | θmax = 26.0°, θmin = 3.4° |
ω scans | h = −7→7 |
Absorption correction: multi-scan (CrysAlis PRO; Agilent, 2014) | k = −23→23 |
Tmin = 0.920, Tmax = 0.990 | l = −17→17 |
7800 measured reflections |