| Bruker APEXII CCD area-detector diffractometer | 1356 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.037 |
| φ and ω scan | θmax = 32.6°, θmin = 2.9° |
| Absorption correction: multi-scan (SADABS; Bruker, 2004) | h = −11→11 |
| Tmin = 0.201, Tmax = 0.201 | k = −9→9 |
| 11674 measured reflections | l = −13→13 |
| 1521 independent reflections |