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. 2016 Feb 6;72(Pt 3):293–296. doi: 10.1107/S2056989016001948
Refinement on F2 Hydrogen site location: difference Fourier map
Least-squares matrix: full Only H-atom coordinates refined
R[F2 > 2σ(F2)] = 0.025 w = 1/[σ2(Fo2) + (0.0195P)2 + 3.6132P] where P = (Fo2 + 2Fc2)/3
wR(F2) = 0.056 (Δ/σ)max < 0.001
S = 1.05 Δρmax = 2.67 e Å3
1521 reflections Δρmin = −2.16 e Å3
82 parameters Extinction correction: SHELXL2014 (Sheldrick, 2015), Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4
1 restraint Extinction coefficient: 0.00067 (18)