| Agilent Xcalibur (Atlas, Gemini) diffractometer | 4036 independent reflections |
| Radiation source: Enhance (Mo) X-ray Source | 2958 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.040 |
| Detector resolution: 10.5564 pixels mm-1 | θmax = 26.1°, θmin = 3.1° |
| ω scans | h = −7→7 |
| Absorption correction: analytical CrysAlis PRO, (Agilent, 2013) | k = −9→9 |
| Tmin = 0.969, Tmax = 0.992 | l = −15→15 |
| 6689 measured reflections |
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