| Agilent Xcalibur (Atlas, Gemini) diffractometer | 2743 independent reflections |
| Radiation source: Enhance (Mo) X-ray Source | 1534 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.058 |
| Detector resolution: 10.5564 pixels mm-1 | θmax = 29.5°, θmin = 3.3° |
| ω scans | h = −28→27 |
| Absorption correction: multi-scan CrysAlis PRO, (Agilent, 2013) | k = −10→9 |
| Tmin = 0.692, Tmax = 1.000 | l = −8→8 |
| 14195 measured reflections |
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