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. 2016 Mar 8;11(3):e0150647. doi: 10.1371/journal.pone.0150647

Fig 1.

Fig 1

Optimized HPLC chromatograms at 220 nm selected from three column system (AI—AIII) and three mobile protocols (BI-BIII). Thirty-one compounds (peaks 1–31) were separated by BIII and identified using UPLC- LTQ Orbitrap mass spectrometry.