Table 4. Recovery of four standards in the extraction of GE (n = 3).
Compounds | Initial amount (mg) | Added amount (mg) | Total recovered amounta (mg) | Recoveryb (%) | RSDc (%) |
---|---|---|---|---|---|
Gastrodin | 1.09 | 0.62 | 1.62 ± 0.01 | 88.02 | 1.26 |
1.09 | 2.24 | 3.35 ± 0.03 | 100.91 | 1.54 | |
1.09 | 3.86 | 4.93 ± 0.01 | 99.65 | 0.30 | |
Parishin E | 1.22 | 0.42 | 1.62 ± 0.02 | 94.65 | 0.57 |
1.22 | 2.04 | 3.33 ± 0.03 | 105.38 | 1.46 | |
1.22 | 4.11 | 5.01 ± 0.03 | 92.15 | 0.70 | |
Parishin B | 1.14 | 0.32 | 1.43 ± 0.00 | 89.88 | 0.52 |
1.14 | 1.72 | 2.88 ± 0.01 | 101.96 | 0.58 | |
1.14 | 3.45 | 4.35 ± 0.00 | 92.85 | 0.13 | |
Parishin | 2.55 | 2.87 | 5.34 ± 0.01 | 97.66 | 0.34 |
2.55 | 8.23 | 10.78 ± 0.02 | 100.43 | 0.00 | |
2.55 | 13.86 | 16.21 ± 0.01 | 98.49 | 0.07 |
a Total recovered amount = mean content ± SD.
b Recovery (%) = (detected amount—original amount)/spiked amount × 100.
c RSD = (recovery SD/mean) × 100