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. 2015 Oct 16;78(2):259–264. doi: 10.1292/jvms.15-0317

Table 3. Accuracy and precision for mycotoxin determination in optimal LC-MS/MS conditions for spiked broiler feed samples.

Mycotoxins Spiking level
(ng/g)
Recovery (%) Intra-day precision
(%RSD)
Inter-day precision
(%RSD)
AFB1 2 96 5.46 6.37
10 98 3.37 5.43
50 101 3.42 3.89
AFB2 2 97 6.38 7.98
10 95 4.43 4.64
50 98 2.21 3.17
AFG1 2 92 3.61 3.77
10 95 4.86 4.22
50 103 2.70 3.45
AFG2 10 91 2.59 2.96
50 96 7.28 7.67
200 88 5.76 7.11
T-2 2 92 6.41 6.11
10 87 5.53 5.79
50 95 3.15 3.48
OTA 2 89 5.13 4.35
10 85 4.64 3.87
50 86 3.79 3.82
ZEA 10 93 3.63 4.05
50 94 5.02 4.69
200 92 1.78 1.98
DON 10 82 5.46 4.86
50 84 3.37 3.51
200 85 3.42 2.89
NIV 10 82 2.51 3.15
50 81 1.87 2.03
200 84 2.27 1.89