Table 3. Accuracy and precision for mycotoxin determination in optimal LC-MS/MS conditions for spiked broiler feed samples.
Mycotoxins | Spiking level (ng/g) |
Recovery (%) | Intra-day precision (%RSD) |
Inter-day precision (%RSD) |
---|---|---|---|---|
AFB1 | 2 | 96 | 5.46 | 6.37 |
10 | 98 | 3.37 | 5.43 | |
50 | 101 | 3.42 | 3.89 | |
AFB2 | 2 | 97 | 6.38 | 7.98 |
10 | 95 | 4.43 | 4.64 | |
50 | 98 | 2.21 | 3.17 | |
AFG1 | 2 | 92 | 3.61 | 3.77 |
10 | 95 | 4.86 | 4.22 | |
50 | 103 | 2.70 | 3.45 | |
AFG2 | 10 | 91 | 2.59 | 2.96 |
50 | 96 | 7.28 | 7.67 | |
200 | 88 | 5.76 | 7.11 | |
T-2 | 2 | 92 | 6.41 | 6.11 |
10 | 87 | 5.53 | 5.79 | |
50 | 95 | 3.15 | 3.48 | |
OTA | 2 | 89 | 5.13 | 4.35 |
10 | 85 | 4.64 | 3.87 | |
50 | 86 | 3.79 | 3.82 | |
ZEA | 10 | 93 | 3.63 | 4.05 |
50 | 94 | 5.02 | 4.69 | |
200 | 92 | 1.78 | 1.98 | |
DON | 10 | 82 | 5.46 | 4.86 |
50 | 84 | 3.37 | 3.51 | |
200 | 85 | 3.42 | 2.89 | |
NIV | 10 | 82 | 2.51 | 3.15 |
50 | 81 | 1.87 | 2.03 | |
200 | 84 | 2.27 | 1.89 |