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. Author manuscript; available in PMC: 2017 Mar 1.
Published in final edited form as: J Chromatogr B Analyt Technol Biomed Life Sci. 2016 Feb 2;1014:56–63. doi: 10.1016/j.jchromb.2016.01.049

Table 3.

Chromsystems external calibrators.



25OHD3
25OHD2
Chromsystems
concentration
(ng/mL)
Measured
Concentration
(ng/mL)
%DEV Chromsystems
concentration
(ng/mL)
Measured
Concentration
(ng/mL)
%DEV


4.50 6.245 38.8 n.d 1.98
9.70 8.967 −7.6 5.00 5.03 2.8
18.50 19.176 3.7 14.30 14.69 2.7
32.90 30.959 −5.9 28.60 27.75 −3.0
65.60 67.321 2.6 57.10 65.56 14.8
102.00 101.078 −0.9 98.60 106.90 8.4
140.00 146.574 4.7 140.00 158.06 12.9


QC (acceptable range 36.0-54.1 ng/mL)
QC (acceptable range 29.6-44.4 ng/mL)
45.1 42.772 37.0 37.25
45.1 48.372 37.0 40.99
45.1 47.769 37.0 38.38
45.1 44.178 37.0 33.37
45.1 47.463 37.0 35.36
%CV = 4.8 %CV = 12.3