Table 1.
Data collection and refinement statistics
| Crystal | TLR8Z-loop |
| Data collection | |
| X-ray source | PF-AR NE3A |
| Wavelength, Å | 1.0000 |
| Space group | R32 |
| Unit cell parameters, Å | |
| a | 171.5 |
| b | 171.5 |
| c | 301.3 |
| Resolution, Å | 2.6 |
| Completeness, % | 100.0 (100.0) |
| Redundancy | 19.5 (19.5) |
| Rmerge, I* | 0.127 (1.146) |
| Average, I/σ(I) | 17.3 (3.1) |
| Refinement | |
| Resolution range, Å | 133.2–2.6 |
| No. of reflections used | 49,947 |
| Model | 1×TLR8 |
| R, %† | 20.6 |
| Rfree, %‡ | 23.9 |
| rmsd | |
| Bond length, Å | 0.012 |
| Bond angles, ° | 1.77 |
Values in parentheses are for the shell with the highest resolution.
*
Rmerge(I) = Σ|I − <I>|/ΣI, where I is the diffraction intensity.
†
R = Σ|Fo − Fc|/ΣFo, where Fo and Fc are the observed and calculated structure amplitudes, respectively.
‡
Rfree is an R value for a 5% subset of all reflections, but was not used in the refinement.