Table 1.
DS | Initial [Ca2+] (mM) | Initial [HxPO4x-3] (mM) | Ca/P molar ratio | Initial [pDNA] (μg/ml) | pDNA- CaP binding efficiency (%) | pH of the precipitating solution | pH of the final solution | Yield (g/dm3) | Average crystallite size (nm) |
---|---|---|---|---|---|---|---|---|---|
12.5 | 125 | 0.1 | 1.25 × 103 | 25 | 25.36 ± 6.56 | 7 | 7 | n.a. | n.a. |
15 | 125 | 0.7 | 178 | 25 | 93.3 ± 0.6 | 7 | 7 | 0.5 | 14.5 (HAp) |
17.5 | 125 | 4.5 | 27.8 | 25 | 99.47 ± 0.92 | 7 | 6.6 | 6 | 15.4 (HAp) |
21 | 125 | 30 | 4.2 | 25 | 97.07 ± 0.61 | 7.3 | 5.8 | 42 | 11.9 (HAp) & 55.4 (DCP) |