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. Author manuscript; available in PMC: 2016 Apr 3.
Published in final edited form as: J Biol Chem. 2006 Sep 29;281(51):39285–39293. doi: 10.1074/jbc.M608758200

Table 1.

Data Collection and Refinement Statistics

Data collection
Space group P6522
Cell dimensions a, b, c (Å) 127.7, 127.7, 206.7
Resolution (Å) 50.0–2.7
Rsym (%) 8.1(71.2)
Mean I/σ(I) 25.4(2.7)
Completeness (%) 97.1(98.4)
Multiplicity 10.1(7.3)
Refinement
Resolution range (Å) 30.0–2.7
Unique reflections 25,906
 Ramachandran statistics 87.1/ 11.7/1.2/0.0
 Rcryst 0.226
 Rfree 0.263
 Number of nonhydrogen atoms (Protein/solvent) 3947/79
R.m.s. deviations from ideal values in
 Bond length (Å) 0.010
 Bond angle (°) 1.235