. 2016 Feb 5;138(12):4105–4119. doi: 10.1021/jacs.5b12974

Table 1. ²H and η̅ Values Determined for Lys Aliphatic Sites in Microcrystalline GB1^a.

For deuterium undergoing large-amplitude motion, η̅ was set to zero for line-shape fitting.

The ¹³Cγ–¹³Cδ and ¹³Cδ−¹³Cξ cross peaks of K4 severely overlap with those of K10. The same ²Hδ and ²Hξ quadrupolar values were assigned to K4 and K10, which were obtained from the overlapped ²H line shapes.

Table 1. 2H and η̅ Values Determined for Lys Aliphatic Sites in Microcrystalline GB1a.

Table 1. ²H and η̅ Values Determined for Lys Aliphatic Sites in Microcrystalline GB1^a.