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. 2016 Mar 16;72(Pt 4):294–299. doi: 10.1107/S2053230X16003599

Table 3. Data collection and processing.

Values in parentheses are for the outer shell.

Diffraction source BL19U1, SSRF
Wavelength (Å) 0.978455
Temperature (K) 100
Detector Pilatus3 6M
Crystal-to-detector distance (mm) 200
Rotation range per image (°) 360
Total rotation range (°) 1.0
Exposure time per image (s) 0.1
Space group P212121
a, b, c (Å) 65.66, 67.26, 93.25
α, β, γ (°) 90, 90, 90
Mosaicity (°) 0.45
Resolution range (Å) 38.32–1.32 (1.39–1.32)
Total No. of reflections 97322
No. of unique reflections 24312
Completeness (%) 99.8 (99.8)
Multiplicity 12.0 (11.2)
I/σ(I)〉 18.4 (3.6)
R r.i.m. (%) 6.6 (65.7)
Overall B factor from Wilson plot (Å2) 15.2