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. 2015 Jul 15;1(5):234–243. doi: 10.1021/acscentsci.5b00163

Figure 2.

Figure 2

Cyclic voltammograms of TEMPO under anaerobic conditions in CH3CN (black trace) and following sequential addition of CF3CO2H (130 mM, red trace) and NaNO2 (2 equiv, blue trace), also under anaerobic conditions. Standard conditions: 10 mM TEMPO, 0.5 M KPF6, N2 atmosphere, scan rate = 10 mV/s, glassy carbon electrode.