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Conversion vs time curves obtained by 1H NMR for the (co)polymerization of HPMA (red circles), GlyMA (black circles), and the overall comonomer mixture (blue circles) at 50 °C using a PGMA56 macro-CTA when targeting diblock copolymer compositions of (a) PGMA56–PHPMA144, (b) PGMA56–P(HPMA130-stat-GlyMA14), and (c) PGMA56–P(HPMA115-stat-GlyMA29). All syntheses were conducted at 15% w/w solids.
