Table 2. Data collection and processing.
Values in parentheses are for the outer shell.
| Diffraction source | ID23-1, ESRF |
| Wavelength (Å) | 0.910 |
| Temperature (K) | 100 |
| Detector | Pilatus 6M |
| Crystal-to-detector distance (mm) | 611.6 |
| Rotation range per image (°) | 0.2 |
| Total rotation range (°) | 191.6 |
| Exposure time per image (s) | 0.07 |
| Space group | C2 |
| a, b, c (Å) | 161.50, 50.40, 65.80 |
| α, β, γ (°) | 90.00, 101.40, 90.00 |
| Mosaicity (°) | 0.496 |
| Resolution range (Å) | 45.77–3.20 (3.30–3.20) |
| Total No. of reflections | 30243 (2660) |
| No. of unique reflections | 8454 (723) |
| Completeness (%) | 95.1 (85.1) |
| Multiplicity | 3.58 (3.68) |
| CC1/2 (%) | 98.9 (74.2) |
| 〈I/σ(I)〉 | 9.17 (2.45) |
| R meas | 0.147 (0.583) |
| Overall B factor from Wilson plot (Å2) | 68.94 |
| Molecules per asymmetric unit | 1 |