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. Author manuscript; available in PMC: 2017 Apr 13.
Published in final edited form as: J Am Chem Soc. 2016 Mar 30;138(14):4962–4971. doi: 10.1021/jacs.6b02032

Table 1.

Increase in reduction yield with increased i-PrOH.

graphic file with name nihms781737u2.jpg
entry additive conversion (%) yield (%) d.r.
1 None 35 17 9.5
2 1 equiv. i-PrOH 51 46 7.4
3 2 equiv. i-PrOH 63 57 7.6
4 5 equiv. i-PrOH 82 76 7.7