Table 1. Characterization of edible silk fibroin coating thickness as a function of dip coating steps and of relative beta-sheet content as a function of exposure time to water annealing.
Number of dip coating processes (x) in silk fibroin suspension [Dx] | Thickness [μDm] |
---|---|
D1 | 27 ±D 8 |
D2 | 32 ±D 7 |
D4 | 35 ±D 8 |
Exposure time to water annealing post-processing [hours] | Silk fibroin coating crystallinity [relative content of beta-sheet structures, %] |
0 | 23 ±D 2 |
1 | 36 ±D 3 |
6 | 48 ±D 4 |
12 | 58 ±D 5 |
No statistically significant difference was found in the coating thickness for increasing number of dip coating steps. The relative beta sheet content of silk fibroin coating was calculated with a previously reported methodology based on the quantification of the relative beta sheets structures in the Amide III absorbance peak collected with ATR-FTIR spectroscopic analysis.