Table 4. Chemical shifts of the H-5 proton resonance in the major and minor isomers of compounds 28 and 29.
compound | triazolyl H-5 resonancea | Δδ ppmb |
---|---|---|
Major isomer of 28 | 8.04 ppm | |
Minor isomer of 28 | 6.91 ppm | |
Z-29 | 7.65 ppm | |
E-29 | 6.54 ppm |
Obtained at 500 MHz in CDCl3;
δ ppm of major isomer – δ ppm of minor isomer.