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. 2016 Mar 1;22(16):5657–5664. doi: 10.1002/chem.201505093

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© 2016 The Authors. Published by Wiley-VCH Verlag GmbH & Co. KGaA.

This is an open access article under the terms of the Creative Commons Attribution License, which permits use, distribution and reproduction in any medium, provided the original work is properly cited.

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Scheme 10 — Reagents and conditions: a) Dess–Martin reagent, CH₂Cl₂; b) but‐3‐en‐1‐ylmagnesium bromide, THF; c) trimethylsilyl trifluoromethanesulfonate (TBSOTf), diisopropylethylamine (DIPEA), CH₂Cl₂; d) Grubbs II (10 mol %), CH₂Cl₂, heating to reflux; e) HCl, EtOH, Et₂O.