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. 2016 Apr 13;27(5):1293–1304. doi: 10.1021/acs.bioconjchem.6b00107

Table 4. Production of Maleimide-PEG6-Ficoll Intermediates at the Bench and Pilot Scales.

Mal-Ficoll lot no. SM-PEG6 linker lot no. Amine/Ficoll molar ratio Maleimide/Ficoll molar ratio
Bench lot 1 Lot A 218 174
Bench lot 2 Lot A 218 162
Bench lot 3 Lot A 218 176
Bench lot 4 Lot A 218 181
Pilot lot 1 Lot A 221 163
Pilot lot 2 Lot A 218 182
Pilot lot 3 Lot A 224 187
Pilot lot 4 Lot B 224 221
Pilot lot 5 Lot B 224 206