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. Author manuscript; available in PMC: 2017 May 20.
Published in final edited form as: J Org Chem. 2016 Mar 22;81(10):3983–3993. doi: 10.1021/acs.joc.5b02580

TABLE 2.

Angles between the Four Planes of Ch, 6-F-Ch, and 5-F-Cha

angle between graphic file with name nihms779091u3.jpg graphic file with name nihms779091u4.jpg graphic file with name nihms779091u5.jpg
A, B 0° 0.9° 1.4°
A, C 0° 1.6° 1.1°
B, C 0° 0.8° 3.7°
B, D 0° 0.9° 1.0°
C, D 0° 0.4° 2.2°
A, D 0° 1.8° 5.9°
estimated error e.s.d 0° 0.4° 0.1°
a

Angles between the planes of 5-F-Ch were calculated from the published X-ray information.17