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(A) HPLC–MS analysis of P. pacificus exometabolome showing ion chromatograms for npar#3 and pasa#9 as well as previously described pasc#9, which is accompanied by two homologues, pasc#12 and pasc#1, with longer fatty acid side chains. In contrast, no homologues of pasa#9 were detected. (B) Analysis of dqfCOSY spectra of P. pacificus metabolome fractions (“natural”) containing pasa#9 and pasy#9 and comparison with spectra of synthetic compounds.
