. 2016 May 24;11(5):e0156117. doi: 10.1371/journal.pone.0156117

Table 4. The results (F-value) of two-way analysis of variance on the effects of vintage and cultivation on volatile compounds in grape berries.

Numbers	Volatile compounds	Vintage	Cultivation	Vintage^*Cultivation
a1	1-pentanol	63.43^**	0.070	.000
a2	2-heptanol	50.28^**	13.04^**	2.9
a3	1-hexanol	0.590	11.49^**	10.42^**
a4	(E)-3-hexen-1-ol	68.64^**	52.73^**	86.79^**
a5	(Z)-3-hexen-1-ol	61.35^**	4.12^*	6.65^*
a6	3-octanol	187.85^*	0.23	0.21
a7	(E)-2-hexen-1-ol	160.92^**	34.65^**	33.12^**
a8	(Z)-2-hexen-1-ol	86.24^**	26.77^**	26.71^**
a9	1-octen-3-ol	553.01^**	414.47^**	391.13^**
a10	1-heptanol	49.95^**	17.68^**	13.58^**
a11	1-octanol	64.22^**	33.65^**	17.75^**
a12	(E)-2-octen-1-ol	80.45^**	6.22^*	0.05
a13	1-dodecanol	368.89^**	0.33	2.24
a14	(Z)-3-nonen-1-ol	8.17^**	4.94^*	0.03
a15	1-decanol	138.01^**	41.67^**	42.79^**
a16	2-nonanol	13.49^**	2.61	2.56
a17	2-octanol	46.59^**	14.25^**	9.1^**
a18	1-butanol	117.82^**	0.55	0.45
a19	hexanal	29.11^**	1.33	0.28
a20	(E)-2-hexenal	1.62	0.89	0.11
a21	octanal	41.69^**	703.1^**	20.62^**
a22	(E)-2-heptenal	196.09^**	2.85	0.61
a23	decanal	6.42^*	0.15	0.08
a24	(E)-2-octenal	136.68^**	0.92	1.51
a25	nononal	308^**	134.31^**	130.85^**
a26	hexanoic acid	22.29^**	0.11	0.15
a27	ethyl hexanoate	432.96^**	303.43^**	302.87^**
a28	hexyl acetate	1182.63^**	926.84^**	918.43^**
a29	(Z)-3-hexen-1-ol, acetate	4.99^*	2.38	1.77
a30	ethyl octanoate	212.63^**	75.79^**	75.51^**
a31	ethyl decanoate	76.67^**	6.83^*	13.51^**
a32	butyl butyrate	1193.62^**	0.02	3.05
b1	styrene	22^**	1.99	0.07
b2	furfural	269.26^**	0.73	0.67
b3	benzaldehyde	23.51^**	160.81^**	36.84^**
b4	5-methyl furfural	0	0.61	0.74
b5	benzylethylaldehy	1.71	1.43	1.17
b6	ethyl benzoate	86.02^**	0.02	0.11
b7	naphthalene	151.63^**	0.55	1.12
b8	TDN	0.12	0.17	4.82^*
b9	ethyl salicylate	13.36^**	0.34	0.34
b10	methyl salicylate	22.91^**	1.8	2.08
b11	benzaldehyde, 3,4-dimethyl	5.37^*	118.3^**	70.82^**
b12	benzyl alcohol	50.38^**	0.05	3.39
b13	aphthalene,1-methyl-	5.34^*	25.46^**	39.4^**
b14	2-phenylethanol	77.92^**	5.25*	7^*
b15	4-methylphenol	191.36^**	10.72^**	10.73^**
b16	2,6-diterbutyl-4-methyl phenol	12.93^**	9.64^**	9.49^**
b17	4-ethyl phenol	226.44^**	4.86^*	2.42
b18	phenol	280.73^**	3.58	7.07^*
c1	2-ethyl-1-hexanol	219.76^**	140.82^**	118.17^**
c2	4-methyl-1-pentanol	45.54^**	22.24^**	20.15^**
c3	IBMP	5.99^*	5.99^*	8.41^**
c4	IPMP	0.63	10.29^**	0.63
d1	β-myrcene	17.44^**	2.79	3.48
d2	D-limonene	63.2^**	47.6^**	46.48^**
d3	p-cymene	7.11^*	3.03	4.72^*
d4	TCH	5.08^*	0.88	1.12
d5	γ-terpinene	2.77	1.73	0.56
d6	terpinolene	74.41^**	0.74	0.74
d7	cis-furan linalool oxide	35.63^**	4.37^*	0.07
d8	trans-furan linalool oxide	27.82^**	77.29^**	49.75^**
d9	nerol oxide	1.6	10.44^**	10.25^**
d10	linalool	21.22^**	3.64	5.03^*
d11	4-terpinenol	12.55^**	2.8	2.58
d12	hotrienol	393.01^**	0.87	5.09^*
d13	β-cyclocitral	22.67^**	1.18	0.8
d14	menthol	16.55^**	14.5^**	12.71^**
d15	α-terpineol	19.89^**	3.72	16.41^**
d16	geranial	200.01^**	0.11	0.06
d17	benzenemethanol	40.01^**	14.94^**	14.94^**
d18	neral	1.95	16.05^**	22.6^**
d19	nerol	7.06^*	0.07	0.08
d20	geraniol	1.98	0.01	0
f1	5-hepten-2-one,6-methyl	10.93^**	0.92	1.78
f2	β-damascenone	13.45^**	0.15	0.34
f3	α-ionone	104.51^**	0.86	0.86
f4	geranylacetone	47.22^**	0.99	1.37
f5	β-ionone	39.16^**	1.06	0.57

** a significance level of p<0.01

* a significance level of p<0.05