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. Author manuscript; available in PMC: 2016 May 27.
Published in final edited form as: Fitoterapia. 2015 May 27;104:80–85. doi: 10.1016/j.fitote.2015.05.017

Table 1.

1H and 13C NMR data for 1 and 4 (in DMSO).

No. 1
δcb 4
δcb
δH (mult; J in Hz)a δH (mult; J in Hz) a
2 4.81 (d, 10.45) 82.7 4.91 (d, 10.8) 83.7
3 4.16 (d, 10.6) 72.9 4.42 (d, 10.72) 72.1
4 189.8 198.0
5 162.2 162.9
6 5.93 (s) 95.5 5.91 (d, 1.8) 96.4
7 164.8 167.2
8 6.08 (s) 93.3 5.86 (d, 1.76) 95.4
9 163.7 163.8
10 102.6 100.9
1′ 127.5 127.7
2′ 6.38 (s) 106.9 6.40 (s) 107.2
3′ 145.8 146.1
4′ 133.4 133.8
5′ 145.8 146.1
6′ 6.38 (s) 106.9 6.38 (s) 107.2
—CH3 3.75 (s) 55.8
a

1H NMR measured at 400 MHz.

b

13C NMR measured at 100 MHz [9].