Table 1.
No. | 1
|
δcb | 4
|
δcb |
---|---|---|---|---|
δH (mult; J in Hz)a | δH (mult; J in Hz) a | |||
2 | 4.81 (d, 10.45) | 82.7 | 4.91 (d, 10.8) | 83.7 |
3 | 4.16 (d, 10.6) | 72.9 | 4.42 (d, 10.72) | 72.1 |
4 | 189.8 | 198.0 | ||
5 | 162.2 | 162.9 | ||
6 | 5.93 (s) | 95.5 | 5.91 (d, 1.8) | 96.4 |
7 | 164.8 | 167.2 | ||
8 | 6.08 (s) | 93.3 | 5.86 (d, 1.76) | 95.4 |
9 | 163.7 | 163.8 | ||
10 | 102.6 | 100.9 | ||
1′ | 127.5 | 127.7 | ||
2′ | 6.38 (s) | 106.9 | 6.40 (s) | 107.2 |
3′ | 145.8 | 146.1 | ||
4′ | 133.4 | 133.8 | ||
5′ | 145.8 | 146.1 | ||
6′ | 6.38 (s) | 106.9 | 6.38 (s) | 107.2 |
—CH3 | 3.75 (s) | 55.8 |
1H NMR measured at 400 MHz.
13C NMR measured at 100 MHz [9].