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. 2016 May 26;72(Pt 3):410–415. doi: 10.1107/S2052520616007058

Table 2. Refinement parameters for the Rietveld refinements performed for the three modifications of In2S3 .

Inline graphic: Bragg Inline graphic factor, Inline graphic: Inline graphic for points with Bragg contribution, Inline graphic: weighted profile R-factor (not corrected for background), Inline graphic: expected R-factor (not corrected for background), Inline graphic: weighted profile R factor (corrected for background), Inline graphic: expected R-factor (corrected for background), Inline graphic: ratio between effective number of reflections and intensity parameters.

    Temperature (K) Inline graphic Inline graphic Inline graphic Inline graphic Inline graphic Inline graphic Inline graphic
#1 β-In2S3 309 10.4 0.014 0.031 0.01 0.049 0.015 5.9
#2 α-In2S3 749 7.9 0.017 0.028 0.01 0.055 0.020 7.3
#3 γ-In2S3 1099 10.8 0.028 0.030 0.01 0.072 0.024 3.8