Table 6. Rietveld quantitative phase analyses of the CQZ_xGl mixtures, where quartz (Q) is the internal standard to used derive the amorphous content (Am), obtained from SXRPD, Mo Kα1 and Cu Kα1 patterns.
The AKLDs for each mixture and the KLD values for the amorphous content are also included.
| Weighed | SXRPD trm | Mo Kα1 trm | Cu Kα1 rfl | |||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| C wt% | Z wt% | Gl wt% | C wt% | Z wt% | Am wt% | AKLD sum | Am KLD | C wt% | Z wt% | Am wt% | AKLD sum | Am KLD | C wt% | Z wt% | Am wt% | AKLD sum | Am KLD | |
| CZQ_0Gl | 50.01 | 49.99 | 0.00 | 49.9 (1) | 49.6 (1) | 0.4 (1) | 0.0050 | – | 47.5 (1) | 49.0 (1) | 3.5 (1) | 0.0358 | – | 47.2 (1) | 40.8 (1) | 12.0 (1) | 0.1305 | – |
| CZQ_2Gl | 48.98 | 48.96 | 2.05 | 49.7 (1) | 49.0 (1) | 1.3 (1) | 0.0169 | 0.009 | 45.9 (1) | 47.7 (1) | 6.4 (1) | 0.0679 | −0.023 | 47.4 (1) | 40.6 (1) | 12.0 (1) | 0.1440 | −0.036 |
| CZQ_4Gl | 47.93 | 47.91 | 4.17 | 47.9 (1) | 47.6 (1) | 4.5 (1) | 0.0066 | −0.003 | 46.5 (1) | 47.0 (1) | 6.5 (1) | 0.0422 | −0.019 | 45.8 (1) | 39.7 (1) | 14.6 (1) | 0.1641 | −0.052 |
| CZQ_8Gl | 46.00 | 46.00 | 7.99 | 46.6 (1) | 45.9 (1) | 7.5 (1) | 0.0120 | 0.005 | 42.6 (1) | 44.8 (1) | 12.5 (1) | 0.0832 | −0.036 | 45.3 (1) | 38.1 (1) | 16.6 (1) | 0.1522 | −0.058 |
| CZQ_16Gl | 41.99 | 41.99 | 16.01 | 42.0 (1) | 41.6 (1) | 16.4 (1) | 0.0079 | −0.004 | 39.9 (1) | 41.7 (1) | 18.5 (1) | 0.0475 | −0.023 | 40.9 (1) | 35.8 (1) | 23.4 (1) | 0.1388 | −0.061 |
| CZQ_32Gl | 34.00 | 34.00 | 31.99 | 34.0 (1) | 33.7 (1) | 32.3 (1) | 0.0061 | −0.003 | 31.7 (1) | 33.1 (1) | 35.2 (1) | 0.0635 | −0.031 | 32.2 (1) | 28.7 (1) | 39.1 (1) | 0.1403 | −0.064 |