(A) Relative ATPase activity of WT yHsp90-His6 and yMps1 mediated phospho-T101-yHsp90-His6. ATPase activity was inhibited by 10 μM GB. Error bars represent SD of three independent experiments. ****p < 0.0001.
(B) Relative ATPase activity of WT hHsp90α-His6 and hMps1 mediated phospho-T115-hHsp90α-His6. ATPase activity was inhibited by 10 μM GB. Error bars represent SD of three independent experiments. ****p < 0.0001.
(C) yHsp90 was isolated from yeast with empty plasmid (C), WT yHsp90-His6 (WT), T101A-yHsp90-His6 (T101A), and T101E-yHsp90-His6 (T101E). Interaction of the co-chaperones yAha1, Cdc37p50, Sba1p23, and Sti1Hop were detected by immunoblotting. Equivalent precipitation of yHsp90 was confirmed by blotting for hexahistidine.
(D) HEK293 cells were transfected with empty plasmid (C), hHsp90α-FLAG (WT), T115A-hHsp90α-FLAG (T115A), or T115E-hHsp90α-FLAG (T115E). Hsp90-FLAG was immunoprecipitated (IP) with anti-FLAG M2 affinity gel and interaction with hAha1 or p50cdc37, p23Sba1, or p60Hop was examined by immunoblotting.