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. Author manuscript; available in PMC: 2016 Nov 1.
Published in final edited form as: J Chem Eng Data. 2015 Nov 17;60(12):3483–3495. doi: 10.1021/acs.jced.5b00751

Table 3.

The as -received purity and the method used to purify the samples further in situ.

chemical name CAS source initial mole fraction purity purification method final mole fraction purity analysis method
naphthalene a
91-20-3
Sigma Aldrich 0.997 vacuum sublimation e PB/PVA < 0.05 Eq. (15)
ferrocene b
102-54-5
Aldrich 0.998 vacuum sublimation e PB/PVA < 0.05 Eq. (15)
diethyl phthalate c
84-66-2
Sigma Aldrich 0.995 cyclic pumping e PB/PVA < 0.05 Eq. (15)
TEMAH d
352535-01-4
SAFC Hitech 0.990 cyclic pumping f 0.03 < PB/PVA < 0.18 Eq. (18)
a

bicyclo[4.4.0]deca-1,3,5,7,9-pentene

b

bis(η 5-cyclopentadienyl)iron

c

diethyl benzene -1,2-dicarboxylate

d

tetrakis(ethylmethylamino)hafnium

e

Bound on PB/PVA obtained from Eq. (15).

f

Range of PB/PVA obtained from fits to Eq. (18).