Table 1.
Composition of PR+: The threading efficiency was calculated based on a presumed 1:2 HPCD:PO unit ratio. # CD refers to the number of HPCD molecules threaded onto the Pluronic core and DMEDA represents umber of DMEDA attached to each PR+ as determined by 1H NMR integration. * Molecular weight estimated from proton NMR integration.
PR+ | # CD | DMEDA | DMEDA/CD | HLBa | Threading Efficiencyb | Mw of PR+ (kDa)c |
---|---|---|---|---|---|---|
F127 | 15 | 63 | 4.2 | 22 | 46% | 42.9 |
L81 | 11 | 95 | 8.6 | 2 | 52% | 32.4 |
L64 | 8 | 71 | 8.8 | 15 | 53% | 23.9 |
F68 | 3 | 10 | 3.3 | 29 | 22% | 19.5 |
L35 | 3 | 20 | 6.6 | 19 | 37% | 11.3 |
HLB (hydrophilic-lipophilic balance) of the copolymers were determined by the manufacturer.
The threading efficiency was calculated based on a presumed 1:2 HPCD:PO unit ratio. # CD refers to the number of HPCD molecules threaded onto the Pluronic core and DMEDA represents umber of DMEDA attached to each PR+ as determined by 1H NMR integration.
Molecular weight estimated from proton NMR integration.