Table 8.
Reaction of benzaldehyde (3a) with indium propiophenone enolate in the CYTOSTM Labsystem (5a/6a in %).
| Entry | Flow rate [mL min−1] | 22 °C | 34 °C | 47 °C | Average rxn. time [min] | |||
| 5a | 6a | 5a | 6a | 5a | 6a | |||
| 1 | 1 | − | − | − | − | − | − | 60 |
| 2 | 2 | 62 | 12 | 59 | 10 | 50 | 14 | 30 |
| 3 | 3 | 63 | 14 | 58 | 14 | 48 | 12 | 20 |
| 4 | 5 | 21 | 12 | 20 | 9 | 12 | 6 | 12 |
| 5 | 9 | 20 | 8 | 22 | 6 | 25 | 5 | 6 |