Table 1.

Optimization of the cross-metathesis reaction between 9 and various alkenes.

Cross-metathesis partners	Conditions used	Isolated yield (%) using catalyst 3	Isolated yield (%) using catalyst 4
10a	DCM, thermal 40 °C, 16 h, 5 mol % catalyst	50	N/Aa
10b	DCM, thermal 40 °C, 16 h, 10 mol % catalyst	14	N/A
	DCM, μ-waveb 60 °C, 60 min, 10 mol % catalyst	N/A	67
10c	DCM, thermal 40 °C, 16 h, 10 mol % catalyst	25	30
	DCM, μ-wave 60 °C, 60 min, 10 mol % catalyst	N/A	30
10d	DCM, thermal 40 °C, 16 h, 10 mol % catalyst	30	40
	DCM, μ-wave 60 °C, 60 min, 10 mol % catalyst	N/A	60

^aN/A: not applicable; ^bμ-wave: microwave.