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. 2016 May 13;6(6):4017–4024. doi: 10.1021/acscatal.6b00321

Figure 2.

Figure 2

In situ Mossbauer spectra of (a) 4Fe after reduction, (b) 4Fe after 20 h TOS, (c) 4FeP after reduction, and (d) 4FeP after 20 h TOS. Reduction: 350 °C, 2 bar, Ar/H2 = 2, 2 h. FTO: 340 °C, 20 bar, H2/CO = 1, TOS = 20 h. (3 Fe sites for Hägg carbide: magenta, red, and purple; 1 Fe site for ε′ carbide: dark cyan; 3–4 Fe sites for Fe1–xO: violet, olive, navy, blue).