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Rietveld refined XRD θ–2θ spectra for SCBRO samples x = 0.10 (a), x = 0.15 (b), and x = 0.20 (c), respectively. The lattice parameters a, b, c, ϕRu-O(1)-Ru, and ϕRu-O(2)-Ru, as evaluated from the Rietveld refinement, as well as refinement reliability coefficient χ2 are marked aside. The full-width at half maximum Δ(2θ) at 2θ = 76.6°, 46.5°, and 22.6°, as a function of x, respectively, are plotted in (d).
