Table 3.
The percentage recoveries of PAHs extraction by C-18 solid-phase with solvent mixture of dichloromethane : hexane (1 : 2).
| PAHs | Amount added (μg/mL) | Retention time | Area | Amount recovered (μg/mL) | % Recovery | % Recovery (mean ± %RSD) |
|---|---|---|---|---|---|---|
| ANT | 5.00 | 18.13 | 30294 | 4.58 | 91.60 | 89.73 ± 1.82 |
| 5.00 | 18.13 | 29865 | 4.45 | 89.00 | ||
| 5.00 | 18.13 | 30867 | 4.43 | 88.60 | ||
|
| ||||||
| FLU | 5.00 | 15.83 | 102408 | 4.90 | 98.00 | 98.60 ± 0.61 |
| 5.00 | 15.82 | 103662 | 4.96 | 99.20 | ||
| 5.00 | 15.83 | 103035 | 4.93 | 98.60 | ||
|
| ||||||
| NAP | 5.00 | 10.47 | 227059 | 4.02 | 80.40 | 81.47 ± 1.16 |
| 5.00 | 10.47 | 231013 | 4.09 | 81.80 | ||
| 5.00 | 10.47 | 232143 | 4.11 | 82.20 | ||
|
| ||||||
| PHE | 5.00 | 18.27 | 32503 | 4.23 | 84.60 | 84.73 ± 1.66 |
| 5.00 | 18.27 | 31580 | 4.17 | 83.40 | ||
| 5.00 | 18.27 | 31438 | 4.31 | 86.20 | ||
|
| ||||||
| PYR | 5.00 | 21.51 | 17145 | 4.77 | 95.40 | 96.07 ± 1.03 |
| 5.00 | 21.51 | 17469 | 4.86 | 97.20 | ||
| 5.00 | 21.51 | 17181 | 4.78 | 95.60 | ||