| Br1—C1 | 1.8848 (13) | C5—C6 | 1.3878 (19) |
| O1—C6 | 1.3655 (18) | C5—H5A | 0.9300 |
| O1—C13 | 1.418 (2) | C7—C12 | 1.3876 (19) |
| O2—C3 | 1.3799 (17) | C7—C8 | 1.4120 (18) |
| O2—C14 | 1.4266 (19) | C8—C9 | 1.3892 (19) |
| O3—C8 | 1.3528 (17) | C9—C10 | 1.408 (2) |
| O3—H3A | 0.72 (3) | C9—C15 | 1.4396 (19) |
| O4—C11 | 1.3464 (18) | C10—C11 | 1.3907 (18) |
| O4—H4A | 0.79 (2) | C10—C16 | 1.434 (2) |
| N1—C15 | 1.137 (2) | C11—C12 | 1.3927 (19) |
| N2—C16 | 1.143 (2) | C12—H12A | 0.9300 |
| C1—C2 | 1.388 (2) | C13—H13A | 0.9600 |
| C1—C6 | 1.3909 (19) | C13—H13B | 0.9600 |
| C2—C3 | 1.3933 (19) | C13—H13C | 0.9600 |
| C2—H2A | 0.9300 | C14—H14A | 0.9600 |
| C3—C4 | 1.3933 (19) | C14—H14B | 0.9600 |
| C4—C5 | 1.4004 (19) | C14—H14C | 0.9600 |
| C4—C7 | 1.4860 (18) | ||
| C6—O1—C13 | 117.15 (12) | C9—C8—C7 | 119.57 (12) |
| C3—O2—C14 | 117.91 (12) | C8—C9—C10 | 121.32 (12) |
| C8—O3—H3A | 108 (2) | C8—C9—C15 | 118.27 (13) |
| C11—O4—H4A | 112.3 (17) | C10—C9—C15 | 120.41 (13) |
| C2—C1—C6 | 121.99 (12) | C11—C10—C9 | 118.94 (12) |
| C2—C1—Br1 | 118.91 (10) | C11—C10—C16 | 119.68 (13) |
| C6—C1—Br1 | 119.09 (10) | C9—C10—C16 | 121.38 (12) |
| C1—C2—C3 | 118.92 (12) | O4—C11—C10 | 117.60 (13) |
| C1—C2—H2A | 120.5 | O4—C11—C12 | 122.95 (12) |
| C3—C2—H2A | 120.5 | C10—C11—C12 | 119.45 (13) |
| O2—C3—C4 | 115.96 (12) | C7—C12—C11 | 122.30 (12) |
| O2—C3—C2 | 123.42 (13) | C7—C12—H12A | 118.8 |
| C4—C3—C2 | 120.62 (12) | C11—C12—H12A | 118.8 |
| C3—C4—C5 | 118.83 (12) | O1—C13—H13A | 109.5 |
| C3—C4—C7 | 123.21 (12) | O1—C13—H13B | 109.5 |
| C5—C4—C7 | 117.87 (12) | H13A—C13—H13B | 109.5 |
| C6—C5—C4 | 121.56 (13) | O1—C13—H13C | 109.5 |
| C6—C5—H5A | 119.2 | H13A—C13—H13C | 109.5 |
| C4—C5—H5A | 119.2 | H13B—C13—H13C | 109.5 |
| O1—C6—C5 | 124.67 (12) | O2—C14—H14A | 109.5 |
| O1—C6—C1 | 117.32 (12) | O2—C14—H14B | 109.5 |
| C5—C6—C1 | 118.01 (13) | H14A—C14—H14B | 109.5 |
| C12—C7—C8 | 118.37 (12) | O2—C14—H14C | 109.5 |
| C12—C7—C4 | 118.74 (11) | H14A—C14—H14C | 109.5 |
| C8—C7—C4 | 122.82 (12) | H14B—C14—H14C | 109.5 |
| O3—C8—C9 | 117.39 (12) | N1—C15—C9 | 179.5 (2) |
| O3—C8—C7 | 122.99 (13) | N2—C16—C10 | 179.4 (2) |
| C13—O1—C6—C1 | 175.14 (15) | C4—C5—C6—O1 | −179.10 (15) |
| C13—O1—C6—C5 | −4.5 (2) | C4—C5—C6—C1 | 1.2 (2) |
| C14—O2—C3—C2 | −1.3 (2) | C4—C7—C8—O3 | −2.4 (2) |
| C14—O2—C3—C4 | 178.48 (15) | C4—C7—C8—C9 | 174.94 (13) |
| Br1—C1—C2—C3 | −178.26 (12) | C12—C7—C8—O3 | −179.24 (14) |
| C6—C1—C2—C3 | 1.0 (2) | C12—C7—C8—C9 | −1.9 (2) |
| Br1—C1—C6—O1 | −2.8 (2) | C4—C7—C12—C11 | −175.62 (13) |
| Br1—C1—C6—C5 | 176.93 (12) | C8—C7—C12—C11 | 1.4 (2) |
| C2—C1—C6—O1 | 177.95 (14) | O3—C8—C9—C10 | 177.94 (14) |
| C2—C1—C6—C5 | −2.4 (2) | O3—C8—C9—C15 | −1.7 (2) |
| C1—C2—C3—O2 | −178.78 (14) | C7—C8—C9—C10 | 0.5 (2) |
| C1—C2—C3—C4 | 1.5 (2) | C7—C8—C9—C15 | −179.13 (13) |
| O2—C3—C4—C5 | 177.70 (14) | C8—C9—C10—C11 | 1.6 (2) |
| O2—C3—C4—C7 | −5.9 (2) | C8—C9—C10—C16 | −178.84 (14) |
| C2—C3—C4—C5 | −2.6 (2) | C15—C9—C10—C11 | −178.81 (14) |
| C2—C3—C4—C7 | 173.88 (14) | C15—C9—C10—C16 | 0.8 (2) |
| C3—C4—C5—C6 | 1.2 (2) | C9—C10—C11—O4 | 177.38 (14) |
| C7—C4—C5—C6 | −175.45 (14) | C9—C10—C11—C12 | −2.1 (2) |
| C3—C4—C7—C8 | 57.1 (2) | C16—C10—C11—O4 | −2.2 (2) |
| C3—C4—C7—C12 | −126.09 (16) | C16—C10—C11—C12 | 178.27 (14) |
| C5—C4—C7—C8 | −126.50 (16) | O4—C11—C12—C7 | −178.82 (14) |
| C5—C4—C7—C12 | 50.37 (19) | C10—C11—C12—C7 | 0.7 (2) |