| Bruker APEXII CCD diffractometer | 4739 reflections with I > 2σ(I) |
| φ and ω scans | Rint = 0.037 |
| Absorption correction: multi-scan (SADABS; Bruker, 2010) | θmax = 34.5°, θmin = 1.7° |
| Tmin = 0.428, Tmax = 0.747 | h = −13→13 |
| 65083 measured reflections | k = −37→37 |
| 6269 independent reflections | l = −12→12 |