| Refinement on F | 0 restraints |
| R[F2 > 2σ(F2)] = 0.039 | 0 constraints |
| wR(F2) = 0.052 | Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.0001F2) |
| S = 2.73 | (Δ/σ)max = 0.015 |
| 3773 reflections | Δρmax = 3.34 e Å−3 |
| 146 parameters | Δρmin = −2.22 e Å−3 |
| Refinement on F | 0 restraints |
| R[F2 > 2σ(F2)] = 0.039 | 0 constraints |
| wR(F2) = 0.052 | Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.0001F2) |
| S = 2.73 | (Δ/σ)max = 0.015 |
| 3773 reflections | Δρmax = 3.34 e Å−3 |
| 146 parameters | Δρmin = −2.22 e Å−3 |